A convenient and mild procedure for the synthesis of alkyl p-toluenesulfinates under solvent-free conditions using microwave irradiation

Abstract

The reactions of aliphatic alcohols with p-toluenesulfinic acid are accelerated by microwave irradiation under solvent-free conditions in the presence of silica gel to afford a high yielding synthesis of p-toluenesulfinate esters.

Microwave Assisted Polycondensation of 4,4'-(Hexafluoroisopro-pylidene) N,N'-bis(phthaloyl-L-leucine) diacid chloride with Aromatic Diols.

Abstract

A new facile and rapid polycondensation reaction of 4,4′-(hexafluoroisopropylidene)-N,N′-bis(phthaloyl-L-leucine) diacid chloride (1) with several aromatic diols such as phenol phthalein (2a), bis phenol-A (2b), 4,4′-hydroquinone (2c), 1,4-dihydroxyanthraquinone (2d), 1,8-dih

Microwave-assisted polycondensation of 4,4′-(hexafluoroisopropylidene)-N,N′-bis(phthaloyl-L-leucine) diacid chloride with aromatic diols

Abstract

A new facile and rapid polycondensation reaction of 4,4′-(hexafluoroisopropylidene)-N,N′-bis(phthaloyl-L-leucine) diacid chloride (1) with several aromatic diols such as phenol phthalein (2a), bis phenol-A (2b), 4,4′-hydroquinone (2c), 1,4-dihydroxyanthraquinone (2d), 1,8-dih