Microwave Heating in Conjunction with Ionic Liquid as a Novel Method for the Fast Synthesis of Optically Active Poly(amide- imide)s Derived from N,N'-(4,4'Hexa fluoroisopropylidenediphthaloyl)-bis-L- methionine and Various Aromatic Diamines

Ionic liquids (IL)s are a new class of solvents which have interesting properties such as

nonvolatility, high ionic concentration, good thermal stability, nonflammability and can

dissolve most of organic as well as inorganic materials. Recently ILs are attracting

more attention due to their significant role in controlling the reaction as a catalyst. It is

important that ILs are the chemicals that can be applied as solvents and catalysts in

green chemistry processes. In this investigation high molecular weight and optically

active poly(amide-imide)s (PAIs) have been synthesized and their properties such as

optical activity, solubility, thermal stability were studied. Polymers were synthesized by

direct polymerization of N,N-(4,4-hexafluoroisopropylidenediphthaloyl)-bis-L-methionine

and various aromatic diamines in the presence of triphenyl phosphite by a new

microwave-assisted ionic liquid (MAIL) method. The compounds obtained were characterized

by elemental C, H and N analysis, solubility, FTIR, 1H NMR. Thermogravimetric

curves were also recorded. All data agree with the proposed structures.

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